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Estimating Pure-Error from Near Replicates in Design of Experiments

Authors

Caleb King (1), Peter Parker (2), Thomas Bzik (3)

Affiliations

(1) JMP Statistical Discovery

(2) NASA

(3) EMD Group

Journal

Journal of Quality Technology, Volume 54, Issue 1

Date Published

2022

Abstract

In design of experiments, setting exact replicates of factor settings enables estimation of pure-error; a model-independent estimate of experimental error useful in communicating inherent system noise and testing model lack-of-fit. Often in practice, the factor levels for replicates are precisely measured rather than precisely set, resulting in near-replicates. This can result in inflated estimates of pure-error due to uncompensated set-point variation. In this article, we review previous strategies for estimating pure-error from near-replicates and propose a simple alternative. We derive key analytical properties and investigate them via simulation. Finally, we illustrate the new approach with an application.

Citation

Caleb King, Thomas Bzik & Peter Parker (2022) Estimating pure-error from near replicates in design of experiments, Journal of Quality Technology, 54:1, 102-117, DOI: 10.1080/00224065.2021.1920347